Category Archives: Toxins

Multiclass cyanotoxin analysis in reservoir waters: Tandem solid-phase extraction followed by zwitterionic hydrophilic interaction liquid chromatography-mass spectrometry.

The presence of cyanobacteria and cyanotoxins in all water bodies, including ocean water and fresh water sources, represents a risk for human health as eutrophication and climate change are enhancing their level of proliferation. For risk assessment and studies on … Continue reading

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Determination of principal ergot alkaloids in swine feeding

Ergot alkaloids are secondary metabolites produced by fungi in the genus Claviceps. They contaminate a large variety of cereals, such as rye, triticale, wheat and barley. The ingestion of contaminated cereals might cause adverse health effects in humans and animals. … Continue reading

Posted in Animal feed, Ergot alkaloids, Mass spectrometry, QuEChERS, RTI2018-097043-B-I00, UHPLC | Tagged , , | Comments Off on Determination of principal ergot alkaloids in swine feeding

Determination of the main ergot alkaloids and their epimers in oat-based functional foods by ultra-high performance liquid chromatography tandem mass spectrometry.

An ultra-high performance liquid chromatography coupled to tandem mass spectrometry method is proposed for the determination of the major ergot alkaloids (ergometrine, ergosine, ergotamine, ergocornine, ergokryptine, ergocristine) and their epimers (ergometrinine, ergosinine, ergotaminine, ergocorninine, ergokryptinine, and ergocristinine) in oat-based foods … Continue reading

Posted in Ergot alkaloids, Mass spectrometry, Mycotoxins, Oat, QuEChERS, RTI2018-097043-B-I00, UHPLC | Tagged , , | Comments Off on Determination of the main ergot alkaloids and their epimers in oat-based functional foods by ultra-high performance liquid chromatography tandem mass spectrometry.

Occurrence of ergot alkaloids in barley and wheat from Algeria

The natural occurrence of six major ergot alkaloids, ergometrine, ergosine, ergotamine, ergocornine, ergokryptine and ergocristine, as well as their corresponding epimers, were investigated in 60 cereal samples (barley and wheat) from Algeria. Ultra-high performance liquid chromatography coupled to tandem mass … Continue reading

Posted in Barley, Ergot alkaloids, Mass spectrometry, Mycotoxins, QuEChERS, RTI2018-097043-B-I00, UHPLC, Wheat | Tagged , , | Comments Off on Occurrence of ergot alkaloids in barley and wheat from Algeria

Multi-mycotoxin occurrence and exposure assessment approach in foodstuffs from Algeria

A survey on 120 cereal samples (barley, maize, rice and wheat) from Algerian markets has been carried out to evaluate the presence of 15 mycotoxins (ochratoxin A, deoxynivalenol, fumonisin B1 and B2, T-2 and HT-2 toxins, zearalenone, fusarenon X, citrinin, … Continue reading

Posted in AGL2015-70708-R, Barley, Maize, Mass spectrometry, Mycotoxins, QuEChERS, Rice, UHPLC, Wheat | Tagged , | Comments Off on Multi-mycotoxin occurrence and exposure assessment approach in foodstuffs from Algeria

Monitoring of cyanotoxins in water from hypersaline microalgae colonies by ultra high performance liquid chromatography with diode array and tandem mass spectrometry detection following salting-out liquid-liquid extraction.

In this study two different analytical approaches have been developed to determine the presence of several cyanotoxins in saline water samples from a continental salt marsh. A salting-out assisted liquid-liquid extraction (SALLE) has been used in combination with ultra-high performance … Continue reading

Posted in Cyanotoxins, Mass spectrometry, RTI2018-097043-B-I00, SALLE, UHPLC, UV-vis, Water | Tagged , , , | Comments Off on Monitoring of cyanotoxins in water from hypersaline microalgae colonies by ultra high performance liquid chromatography with diode array and tandem mass spectrometry detection following salting-out liquid-liquid extraction.

Plant-based milks: unexplored source of emerging mycotoxins. A proposal for the control of enniatins and beauvericin using UHPLC-MS/MS

Mycotoxins have become one of the most common contaminants reported worldwide. Current legislation has established maximum levels only for some well-known mycotoxins; however, there are many other “emerging mycotoxins” for which there is no regulation, as enniatins and beauvericin. An … Continue reading

Posted in AGL2015-70708-R, Enniatins, Mass spectrometry, SALLE, UHPLC, Vegetable milks | Tagged , , | Comments Off on Plant-based milks: unexplored source of emerging mycotoxins. A proposal for the control of enniatins and beauvericin using UHPLC-MS/MS

Occurrence of mycotoxins in swine feeding from Spain.

A survey including 228 pig feed samples from Spain has been developed, exploring the occurrence of 19 mycotoxins (aflatoxins B1, B2, G1 and G2, ochratoxin A, fumonisins B1 and B2, citrinin, zearalenone, deoxynivalenol, fusarenon X, sterigmatocystin, T-2 toxin, HT-2 toxin, … Continue reading

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Aspergillus section Flavi and aflatoxins in dried figs and nuts in Algeria

The presence of Aspergillus section Flavi and aflatoxin (AF) contamination was investigated in 112 samples of peanuts, almonds and dried figs collected in Algeria. The occurrence of aflatoxin B1 (AFB1), B2 (AFB2), G1 (AFG1) and G2 (AFG2) in different commodities has been determined with … Continue reading

Posted in AGL2015-70708-R, Aflatoxins, Dried fruit, HPLC, Mycotoxins, Nuts, Photo-induced, Solid-liquid extraction | Tagged , | Comments Off on Aspergillus section Flavi and aflatoxins in dried figs and nuts in Algeria

Determination of Fusarium toxins in functional vegetable milks applying salting-out-assisted liquid–liquid extraction combined with ultra-high-performance liquid chromatography tandem mass spectrometry

Vegetable milks are considered as functional foods due to their physiological benefits. Although the consumption of these products has significantly increased, they have received little attention in legislation with regard to contaminants. However, they may contain mycotoxins resulting from the … Continue reading

Posted in AGL2015-70708-R, Mass spectrometry, Mycotoxins, SALLE, UHPLC, Vegetable milks | Tagged , , | Comments Off on Determination of Fusarium toxins in functional vegetable milks applying salting-out-assisted liquid–liquid extraction combined with ultra-high-performance liquid chromatography tandem mass spectrometry