Category Archives: P12-AGR-1647

Collision cross section (CCS) as a complementary parameter to characterize human and veterinary drugs

Posted on 5 November, 2018 by fqm302

In the context of human and veterinary drugs identification, ion mobility spectrometry (IMS) in combination with mass spectrometry (MS) may provide a relevant complementary piece of information to mass-to-charge ratio (m/z), the so-called collision-cross-section (CCS). Up to now, however, the … Continue reading →

Posted in AGL2015-70708-R, Benzimidazoles, Ion mobility, P12-AGR-1647 | Comments Off on Collision cross section (CCS) as a complementary parameter to characterize human and veterinary drugs

Development and validation of a QuEChERS method for the analysis of 5-nitroimidazole traces in infant milk-based samples by ultra-high performance liquid chromatography-tandem mass spectrometry

Posted on 14 June, 2018 by fqm302

QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) methodology in combination with UHPLC–MS/MS is proposed for the determination of 5-nitroimidazole (5-NDZ) residues in infant milk-based products. Chromatographic separation was accomplished in a C18 Zorbax Eclipse Plus RRHD (50 × 2.1 mm, 1.8 μm) column … Continue reading →

Posted in 5-nitroimidazoles, AGL2015-70708-R, Infant foods, Mass spectrometry, P12-AGR-1647, QuEChERS, UHPLC | Tagged , , | Comments Off on Development and validation of a QuEChERS method for the analysis of 5-nitroimidazole traces in infant milk-based samples by ultra-high performance liquid chromatography-tandem mass spectrometry

Green and simple analytical method to determine benzimidazoles in milk samples by using salting-out assisted liquid-liquid extraction and capillary liquid chromatography

Posted on 29 May, 2018 by fqm302

A green and simple multiresidue method using capillary liquid chromatography (CLC) with UV-diode array detection (DAD) has been developed for the determination of sixteen benzimidazoles (BZs) and its metabolites in milk samples. The separation was achieved in <32 min, using a … Continue reading →

Posted in AGL2015-70708-R, Benzimidazoles, Capillary HPLC, Milk, P12-AGR-1647, SALLE, UV-vis | Tagged , , | Comments Off on Green and simple analytical method to determine benzimidazoles in milk samples by using salting-out assisted liquid-liquid extraction and capillary liquid chromatography

Ultra-high performance liquid chromatography with fluorescence detection following salting-out assisted liquid–liquid extraction for the analysis of benzimidazole residues in farm fish samples

Posted on 14 March, 2018 by fqm302

Ultra-high performance liquid chromatography (UHPLC) coupled with fluorescence detection (FL) has been proposed for the first time to determine thirteen benzimidazoles (BZs) in farmed fish samples. In order to optimize the chromatographic separation, parameters such as mobile phase composition and … Continue reading →

Posted in AGL2015-70708-R, Anthelmintic, Aquaculture products, Benzimidazoles, Fluorescence, P12-AGR-1647, SALLE, Sea bass, Sea bream, Trout, UHPLC | Tagged , , | Comments Off on Ultra-high performance liquid chromatography with fluorescence detection following salting-out assisted liquid–liquid extraction for the analysis of benzimidazole residues in farm fish samples

Simple and rapid determination of 5-nitroimidazoles and metabolites in fish roe samples by salting-out assisted liquid-liquid extraction and UHPLC-MS/MS.

Posted on 23 February, 2018 by fqm302

A novel multiresidue method is proposed for the determination of 12 5-nitroimidazoles and their metabolites in fish roe samples using UHPLC-MS/MS. A salting-out assisted liquid-liquid extraction procedure was performed prior to sample analysis. The separation of compounds was accomplished using … Continue reading →

Posted in 5-nitroimidazoles, Fish roe, Mass spectrometry, P12-AGR-1647, SALLE, UHPLC | Tagged , , | Comments Off on Simple and rapid determination of 5-nitroimidazoles and metabolites in fish roe samples by salting-out assisted liquid-liquid extraction and UHPLC-MS/MS.

Determination of tetracyclines in human urine samples by capillary electrophoresis in combination with field amplified sample injection.

Posted on 9 November, 2017 by fqm302

A sensitive method using CZE‐UV detection has been developed for the determination of five tetracycline antibiotics in human urine samples. To improve the sensitivity of the method, an on‐line preconcentration strategy, named field‐amplified sample injection, has been developed, based on … Continue reading →

Posted in CZE, Dilute and shoot, FASI, P12-AGR-1647, Tetracyclines, UV-vis, Urine | Tagged , | Comments Off on Determination of tetracyclines in human urine samples by capillary electrophoresis in combination with field amplified sample injection.

Evaluation of a selective approach for the determination of 5-nitroimidazoles in aquaculture products by capillary liquid chromatography using molecularly imprinted solid-phase extraction

Posted on 6 November, 2017 by fqm302

Capillary liquid chromatography with UV detection is proposed for the determination of 5-nitroimidazole residues in aquaculture products. The separation was carried out in a C18 column at 20 °C, using a mobile phase consisting of water and acetonitrile, at 7 μL/min and … Continue reading →

Posted in 5-nitroimidazoles, Aquaculture products, Capillary HPLC, Crab, MIPs, P12-AGR-1647, Prawn, Salmon, Velvet swimming crab | Tagged , , | Comments Off on Evaluation of a selective approach for the determination of 5-nitroimidazoles in aquaculture products by capillary liquid chromatography using molecularly imprinted solid-phase extraction

A high-throughput UHPLC method for the analysis of 5-nitroimidazole residues in milk based on salting-out assisted liquid–liquid extraction.

Posted on 26 October, 2017 by fqm302

A novel salting-out assisted liquid–liquid extraction (SALLE) method has been developed for the extraction of eight 5-NDZ antibiotics from milk samples prior to their analysis by UHPLC. An exhaustive study of the parameters involved in the SALLE procedure has been … Continue reading →

Posted in 5-nitroimidazoles, Milk, P12-AGR-1647, SALLE, UHPLC, UV-vis | Tagged , , | Comments Off on A high-throughput UHPLC method for the analysis of 5-nitroimidazole residues in milk based on salting-out assisted liquid–liquid extraction.

Coupling sweeping-micellar electrokinetic chromatography with tandem mass spectrometry for the therapeutic monitoring of benzimidazoles in animal urine by dilute and shoot.

Posted on 2 August, 2017 by fqm302

A new method based on micellar electrokinetic chromatography-tandem mass spectrometry (MEKC-MS/MS) has been developed for the identification and simultaneous quantification of thirteen benzimidazoles in animal urine. In order to obtain an appropriate separation with the highest sensitivity, different electrophoretic parameters … Continue reading →

Posted in Anthelmintic, Benzimidazoles, Biological fluids, Dilute and shoot, Electrophoresis, MEKC, Mass spectrometry, P12-AGR-1647, Sweeping, Urine | Tagged , , | Comments Off on Coupling sweeping-micellar electrokinetic chromatography with tandem mass spectrometry for the therapeutic monitoring of benzimidazoles in animal urine by dilute and shoot.

Characterization of carbamate pesticides in natural water from Cameroon.

Posted on 19 July, 2017 by fqm302

With the increased use of chemicals in agriculture for crop protection and improvement of yield, the contamination of water is currently a serious health concern. This study used solid-phase extraction with ultra-high-performance liquid chromatography–tandem mass spectrometry to evaluate the presence … Continue reading →

Posted in Carbamates, Mass spectrometry, P12-AGR-1647, Pesticides, SPE, UHPLC, Water | Tagged , , | Comments Off on Characterization of carbamate pesticides in natural water from Cameroon.