Category Archives: Vegetables

Capillary electrophoresis tandem mass spectrometry to determine multiclass cyanotoxins in reservoir water and spinach samples.

Cyanotoxins constitute a group of toxic secondary metabolites, the presence of which in any water body poses a major health risk. Moreover, advanced organisms such as edible plants exposed to these toxins, are a possible pathway for human exposure. Green … Continue reading

Posted in CZE, Cyanotoxins, FASS, Mass spectrometry, PID2021-127804OB-I00, SPE, Spinach, Water, acid barrage, pH-junction | Tagged , , , | Comments Off on Capillary electrophoresis tandem mass spectrometry to determine multiclass cyanotoxins in reservoir water and spinach samples.

Evaluation of direct analysis in real time for the determination of highly polar pesticides in lettuce and celery using modified Quick Polar Pesticides Extraction method

Direct analysis in real time (DART) was evaluated for the determination of a number of highly polar pesticides using the Quick Polar Pesticides Extraction (QuPPe) method. DART was hyphenated to high resolution mass spectrometry (HRMS) in order to get the … Continue reading

Posted in AGL2015-70708-R, Celery, DART, Lettuce, Polar, QuPPe | Tagged , | Comments Off on Evaluation of direct analysis in real time for the determination of highly polar pesticides in lettuce and celery using modified Quick Polar Pesticides Extraction method

QuEChERS-based method for the determination of carbamate residues in aromatic herbs by UHPLC-MS/MS

A new reliable, fast and highly sensitive method based on ultra-high performance liquid chromatography tandem mass spectrometry has been developed and validated for the determination of 28 carbamates in aromatic herbs. A modified QuEChERS-based method was optimized for the extraction … Continue reading

Posted in AGL2015-70708-R, Aromatic herbs, Carbamates, Mass spectrometry, QuEChERS, UHPLC | Tagged | Comments Off on QuEChERS-based method for the determination of carbamate residues in aromatic herbs by UHPLC-MS/MS

Multiclass mycotoxin analysis in Silybum marianum by ultra high performance liquid chromatography–tandem mass spectrometry using a procedure based on QuEChERS and dispersive liquid–liquid microextraction

Ultra high performance liquid chromatography–tandem mass spectrometry (UHPLC–MS/MS) has been proposed for the determination of 15 mycotoxins in milk thistle (Silybum marianum), including aflatoxins, fumonisins, trichothecenes, ochratoxin A, citrinin, sterigmatocystin and zearalenone. The mycotoxins were detected by electrospray ionization in … Continue reading

Posted in DLLME, Mass spectrometry, Milk thistle, Mycotoxins, QuEChERS, UHPLC | Tagged | Comments Off on Multiclass mycotoxin analysis in Silybum marianum by ultra high performance liquid chromatography–tandem mass spectrometry using a procedure based on QuEChERS and dispersive liquid–liquid microextraction

Determination of carbamates at trace levels in water and cucumber by capillary liquid chromatography

A sensitive and reliable method using capillary HPLC with UV-diode array detection (DAD) has been developed and validated for trace determination of carbamate pesticides in cucumber and environmental water samples. The analytes, including carbofuran, carbaryl, methiocarb, promecarb, benthiocarb and fenoxycarb, … Continue reading

Posted in Capillary HPLC, Carbamates, Chromatography, Food, Pesticides, SPE, UV-vis, Vegetables, Water | Comments Off on Determination of carbamates at trace levels in water and cucumber by capillary liquid chromatography