Category Archives: Neonicotinoids

Analytical methods based on liquid chromatography and capillary electrophoresis to determine neonicotinoid residues in complex matrices. A comprehensive review.

Neonicotinoids (NNIs) are neuro-active and systemic insecticides widely used to protect crops from pest attack. During the last decades, there has been an increase concern about their uses and toxic effects, especially to beneficial and non-target insects such as pollinators. … Continue reading

Posted in B-AGR-202-UGR20, Chromatography, Electrophoresis, Neonicotinoids, Review | Tagged | Comments Off on Analytical methods based on liquid chromatography and capillary electrophoresis to determine neonicotinoid residues in complex matrices. A comprehensive review.

Sweeping-micellar electrokinetic chromatography with tandem mass spectrometry as an alternative methodology to determine neonicotinoid and boscalid residues in pollen and honeybee samples.

In this work, it is proposed for the first time an electrophoretic approach based on micellar electrokinetic chromatography coupled with tandem mass spectrometry (MEKC-MS/MS) for the simultaneous determination of nine neonicotinoids (NNIs) together with the fungicide boscalid in pollen and … Continue reading

Posted in B-AGR-202-UGR20, EQC2018-004453-P, Honeybees, Insects, MEKC, Mass spectrometry, Neonicotinoids, Pesticides, Pollen, QuEChERS, RED2018-102522-T, RTI2018-097043-B-I00, Sweeping | Tagged , , , | Comments Off on Sweeping-micellar electrokinetic chromatography with tandem mass spectrometry as an alternative methodology to determine neonicotinoid and boscalid residues in pollen and honeybee samples.

Capillary liquid chromatography as an effective method for the determination of seven neonicotinoid residues in honey samples

A new analytical method based on capillary liquid chromatography with diode array detection has been developed for the simultaneous quantification of seven neonicotinoid insecticides commercially available (imidacloprid, thiacloprid, clothianidin, thiamethoxam, acetamiprid, nitenpyram, and dinotefuran) in honey samples. The separation was … Continue reading

Posted in AGL2015-70708-R, Capillary HPLC, DLLME, Honey, Neonicotinoids, UV-vis | Tagged , , | Comments Off on Capillary liquid chromatography as an effective method for the determination of seven neonicotinoid residues in honey samples

Micellar electrokinetic chromatography as efficient alternative for the multiresidue determination of seven neonicotinoids and 6-chloronicotinic acid in environmental samples

A simple, sensitive, and efficient method has been developed for the determination of the seven neonicotinoid insecticides commercially available (imidacloprid, thiacloprid, clothianidin, thiamethoxam, acetamiprid, nitenpyram, and dinotefuran) and the main metabolite 6-chloronicotinic acid. Micellar electrokinetic chromatography (MEKC) mode was applied, … Continue reading

Posted in AGL2015-70708-R, MEKC, Neonicotinoids, SPE, Soil, Solid-liquid extraction, UV-vis, Water | Tagged , , | Comments Off on Micellar electrokinetic chromatography as efficient alternative for the multiresidue determination of seven neonicotinoids and 6-chloronicotinic acid in environmental samples