Category Archives: HPLC

A natural deep eutectic solvent as a novel dispersive solvent in dispersive liquid-liquid microextraction based on solidification of floating organic droplet for the determination of pesticide residues.

Current trends in analytical chemistry encourage the use of innocuous solvents to develop modern methods aligned with green chemistry. In this sense, natural deep eutectic solvents (NADESs) have emerged as a novel generation of green solvents which can be employed … Continue reading

Posted in Fipronil, HPLC, NADES, RED2018-102522-T, UV-vis, Water, Wine | Tagged , | Comments Off on A natural deep eutectic solvent as a novel dispersive solvent in dispersive liquid-liquid microextraction based on solidification of floating organic droplet for the determination of pesticide residues.

Aspergillus section Flavi and aflatoxins in dried figs and nuts in Algeria

The presence of Aspergillus section Flavi and aflatoxin (AF) contamination was investigated in 112 samples of peanuts, almonds and dried figs collected in Algeria. The occurrence of aflatoxin B1 (AFB1), B2 (AFB2), G1 (AFG1) and G2 (AFG2) in different commodities has been determined with … Continue reading

Posted in AGL2015-70708-R, Aflatoxins, Dried fruit, HPLC, Mycotoxins, Nuts, Photo-induced, Solid-liquid extraction | Tagged , | Comments Off on Aspergillus section Flavi and aflatoxins in dried figs and nuts in Algeria

Use of onion extract as a dairy cattle feed supplement: monitoring propyl propane thiosulfonate as a marker of its effect on milk attributes.

Onion extract is used as a feed supplement for the diet of dairy cows, acting as inhibitor of methane production; however, its properties could alter sensory attributes of milk. In this work, we propose a method to evaluate the influence … Continue reading

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Development of magnetic molecularly imprinted polymers for selective extraction: determination of citrinin in rice samples by liquid chromatography with UV diode array detection.

In this work, we report the synthesis of novel magnetic molecularly imprinted polymers (m-MIPs) and their application to the selective extraction of the mycotoxin citrinin (CIT) from food samples. The polymers were prepared by surface imprinting of Fe3O4 nanoparticles, using … Continue reading

Posted in HPLC, MIPs, Mycotoxins, Rice, UV-vis | Comments Off on Development of magnetic molecularly imprinted polymers for selective extraction: determination of citrinin in rice samples by liquid chromatography with UV diode array detection.

Determination of aflatoxins in yogurt by dispersive liquid – liquid microextraction and HPLC with photo-induced fluorescence detection.

A high-performance liquid chromatography (HPLC) method with fluorescence detection for the determination of aflatoxins B1, B2, G1, G2, and M1 in yogurt using dispersive liquid–liquid microextraction as alternative sample treatment has been developed. To enhance the fluorescence of aflatoxins B1 … Continue reading

Posted in AGL2015-70708-R, Aflatoxins, DLLME, HPLC, P12-AGR-1647, Photo-induced, Yogurt | Tagged , | Comments Off on Determination of aflatoxins in yogurt by dispersive liquid – liquid microextraction and HPLC with photo-induced fluorescence detection.