Category Archives: Food

On-line preconcentration for the determination of aflatoxins in rice samples by micellar electrokinetic capillary chromatography with laser induced fluorescence detection

Posted on 30 June, 2010 by fqm302

MEKC coupling with LIF detection has been used for the determination of four aflatoxins (B1, B2, G1 and G2). Separations were performed in an uncoated fused-silica capillary (70 cm×75 μm id, 55 cm effective length), using 20 mM borate buffer with 30 mM SDS (pH … Continue reading →

Posted in Fluorescence, LIF, MEKC, Mycotoxins, Rice, Stacking | Tagged | Comments Off on On-line preconcentration for the determination of aflatoxins in rice samples by micellar electrokinetic capillary chromatography with laser induced fluorescence detection

Trace determination of sulfonylurea herbicides in water and grape samples by capillary zone electrophoresis using large volume sample stacking

Posted on 23 May, 2010 by fqm302

A sensitive and reliable method using capillary zone electrophoresis with UV-diode array detection has been developed and validated for trace determination of residues of sulfonylurea herbicides in environmental water samples and grapes from different origins. The analytes included are triasulfuron, … Continue reading →

Posted in CZE, Electrophoresis, Food, Fruit, Pesticides, Stacking, Sulfonylurea, UV-vis, Water | Tagged | Comments Off on Trace determination of sulfonylurea herbicides in water and grape samples by capillary zone electrophoresis using large volume sample stacking

Laser induced fluorescence coupled to capillary electrophoresis for the determination of fluoroquinolones in foods of animal origin using molecularly imprinted polymers

Posted on 17 February, 2010 by fqm302

A method for the simultaneous determination of four fluoroquinolones of veterinary use (ciprofloxacin, danofloxacin, enrofloxacin and sarafloxacin) in two complex matrixes, such as bovine raw milk and pig kidney, has been established and validated. The method is based on the … Continue reading →

Posted in Antibiotics, CZE, Electrophoresis, Fluorescence, Food, LIF, MIPs, Milk, Pig kidney, Quinolones, Sample treatment | Tagged | Comments Off on Laser induced fluorescence coupled to capillary electrophoresis for the determination of fluoroquinolones in foods of animal origin using molecularly imprinted polymers