Categories
- Amino acids (2)
- Animal feed (5)
- PTSO (3)
- Anthelmintic (6)
- Benzimidazoles (6)
- Antibiotics (31)
- 5-nitroimidazoles (10)
- Aminoglycosides (2)
- Quinolones (8)
- Sulfonamides (2)
- Tetracyclines (6)
- β-lactams (5)
- Cephalosporins (3)
- Biological fluids (11)
- Human serum (1)
- Pig serum (2)
- Urine (8)
- Biomonitoring (1)
- C4D (1)
- Chemiluminescence (6)
- Photoinduced (2)
- Chromatography (57)
- Capillary HPLC (12)
- GC (1)
- HILIC (4)
- HPLC (5)
- UHPLC (32)
- Contaminants (2)
- Cyclodextrins (1)
- DART (1)
- Drugs (8)
- Anaesthetics (1)
- Muscle relaxants (1)
- Steroids (1)
- Electrochromatography (1)
- Electrophoresis (39)
- Fingerprints (1)
- Flow injection analysis (1)
- Fluorescence (15)
- LIF (7)
- Photo-induced (3)
- Food (63)
- Aquaculture products (4)
- Barley (4)
- Cheese (1)
- Eggs (4)
- Fruit (2)
- Dried fruit (1)
- Honey (3)
- Infant foods (2)
- Juice (3)
- Maize (3)
- Meat (4)
- Chicken muscle (1)
- Pig kidney (1)
- Pork muscle (1)
- Milk (12)
- Nuts (2)
- Oat (2)
- Pseudocereals (1)
- Rice (6)
- Seeds (2)
- Spelt (1)
- Supplements (4)
- Blue-green algae (1)
- Pollen (1)
- Propolis (1)
- Royal jelly (1)
- Vegetable milks (2)
- Vegetables (5)
- Aromatic herbs (1)
- Celery (1)
- Lettuce (1)
- Milk thistle (1)
- Spinach (1)
- Wheat (7)
- Durum wheat (1)
- Wine (4)
- Yogurt (2)
- Insects (1)
- Honeybees (1)
- Ionic liquids (1)
- Mass spectrometry (49)
- Ion mobility (4)
- Metabolites (1)
- Destruxins (1)
- Metabolomics (3)
- Pesticides (21)
- Carbamates (9)
- Fipronil (3)
- Neonicotinoids (4)
- Polar (1)
- Sulfonylurea (3)
- Pharmaceutical formulations (1)
- Plants (1)
- Potato plant (1)
- Projects (59)
- AGL2015-70708-R (21)
- B-AGR-202-UGR20 (4)
- EQC2018-004453-P (2)
- P12-AGR-1647 (26)
- PID2020–120020RA-I00 (3)
- PID2021-127804OB-I00 (4)
- PROYEXCEL_00195 (3)
- RED2018-102522-T (2)
- RTI2018-097043-B-I00 (9)
- Review (10)
- Sample treatment (84)
- DLLME (16)
- Dilute and shoot (2)
- Hollow-fiber liquid-phase microextraction (1)
- Liquid-liquid extraction (1)
- MIPs (8)
- NADES (1)
- QuEChERS (22)
- QuPPe (1)
- SALLE (15)
- SPE (16)
- Solid-liquid extraction (4)
- UASEME (1)
- automated SPE (1)
- on-line SPE (1)
- Sequential injection analysis (1)
- Soil (1)
- Theses (5)
- Toxins (28)
- Cyanotoxins (4)
- Mycotoxins (24)
- Aflatoxins (4)
- Enniatins (2)
- Ergot alkaloids (4)
- Trabajo fin máster (2)
- UV-vis (29)
- Water (21)
- Wastewater (1)
Archives
- April 2024
- January 2024
- December 2023
- October 2023
- September 2023
- August 2023
- July 2023
- February 2023
- September 2022
- April 2022
- November 2021
- September 2021
- July 2021
- June 2021
- April 2021
- December 2020
- October 2020
- August 2020
- April 2020
- March 2020
- February 2020
- December 2019
- July 2019
- June 2019
- February 2019
- November 2018
- October 2018
- September 2018
- June 2018
- May 2018
- March 2018
- February 2018
- November 2017
- October 2017
- August 2017
- July 2017
- June 2017
- May 2017
- April 2017
- March 2017
- February 2017
- January 2017
- December 2016
- November 2016
- September 2016
- August 2016
- July 2016
- May 2016
- March 2016
- February 2016
- December 2015
- November 2015
- August 2015
- October 2013
- September 2013
- August 2013
- July 2013
- May 2013
- February 2013
- January 2013
- December 2012
- November 2012
- August 2012
- July 2012
- June 2012
- February 2012
- December 2011
- November 2011
- September 2011
- July 2011
- April 2011
- September 2010
- July 2010
- June 2010
- May 2010
- April 2010
- February 2010
- January 2010
-
Recent Posts
- Assessing human exposure to pesticides and mycotoxins: optimization and validation of a method for multianalyte determination in urine samples.
- Capillary electrophoresis tandem mass spectrometry to determine multiclass cyanotoxins in reservoir water and spinach samples.
- Determination of bile acids in serum of pigs exposed to polychlorinated biphenyls by liquid chromatography-mass spectrometry.
- Mycotoxin occurrence in milk and durum wheat samples from Tunisia using dispersive liquid–liquid microextraction and liquid chromatography with fluorescence detection.
- Deeper insights into the effects of low dietary levels of polychlorinated biphenyls on pig metabolism using gas chromatography-high resolution mass spectrometry metabolomics.
Tags
Category Archives: Sample treatment
Determination of tetracyclines in human urine samples by capillary electrophoresis in combination with field amplified sample injection.
A sensitive method using CZE‐UV detection has been developed for the determination of five tetracycline antibiotics in human urine samples. To improve the sensitivity of the method, an on‐line preconcentration strategy, named field‐amplified sample injection, has been developed, based on … Continue reading
Posted in CZE, Dilute and shoot, FASI, P12-AGR-1647, Tetracyclines, UV-vis, Urine
Tagged CE, UV-Vis
Comments Off on Determination of tetracyclines in human urine samples by capillary electrophoresis in combination with field amplified sample injection.
Evaluation of a selective approach for the determination of 5-nitroimidazoles in aquaculture products by capillary liquid chromatography using molecularly imprinted solid-phase extraction
Capillary liquid chromatography with UV detection is proposed for the determination of 5-nitroimidazole residues in aquaculture products. The separation was carried out in a C18 column at 20 °C, using a mobile phase consisting of water and acetonitrile, at 7 μL/min and … Continue reading
Posted in 5-nitroimidazoles, Aquaculture products, Capillary HPLC, Crab, MIPs, P12-AGR-1647, Prawn, Salmon, Velvet swimming crab
Tagged MIPs, UV-Vis, µHPLC
Comments Off on Evaluation of a selective approach for the determination of 5-nitroimidazoles in aquaculture products by capillary liquid chromatography using molecularly imprinted solid-phase extraction
Determination of Fusarium toxins in functional vegetable milks applying salting-out-assisted liquid–liquid extraction combined with ultra-high-performance liquid chromatography tandem mass spectrometry
Vegetable milks are considered as functional foods due to their physiological benefits. Although the consumption of these products has significantly increased, they have received little attention in legislation with regard to contaminants. However, they may contain mycotoxins resulting from the … Continue reading
Posted in AGL2015-70708-R, Mass spectrometry, Mycotoxins, SALLE, UHPLC, Vegetable milks
Tagged MS, SALLE, UHPLC
Comments Off on Determination of Fusarium toxins in functional vegetable milks applying salting-out-assisted liquid–liquid extraction combined with ultra-high-performance liquid chromatography tandem mass spectrometry
Simple determination of aflatoxins in rice by ultra-high performance liquid chromatography coupled to chemical post-column derivatization and fluorescence detection
A fast and simple analytical method was developed and characterized for the determination of aflatoxins (B1, B2, G1 and G2) in rice. The procedure is based on a simple solid-liquid extraction without further clean-up, and analysis by ultra-high performance liquid … Continue reading
Posted in AGL2015-70708-R, Aflatoxins, Fluorescence, Rice, Solid-liquid extraction, UHPLC
Tagged Fluorescence, UHPLC
Comments Off on Simple determination of aflatoxins in rice by ultra-high performance liquid chromatography coupled to chemical post-column derivatization and fluorescence detection
A high-throughput UHPLC method for the analysis of 5-nitroimidazole residues in milk based on salting-out assisted liquid–liquid extraction.
A novel salting-out assisted liquid–liquid extraction (SALLE) method has been developed for the extraction of eight 5-NDZ antibiotics from milk samples prior to their analysis by UHPLC. An exhaustive study of the parameters involved in the SALLE procedure has been … Continue reading
Posted in 5-nitroimidazoles, Milk, P12-AGR-1647, SALLE, UHPLC, UV-vis
Tagged HPLC, SALLE, UV-Vis
Comments Off on A high-throughput UHPLC method for the analysis of 5-nitroimidazole residues in milk based on salting-out assisted liquid–liquid extraction.
Coupling sweeping-micellar electrokinetic chromatography with tandem mass spectrometry for the therapeutic monitoring of benzimidazoles in animal urine by dilute and shoot.
A new method based on micellar electrokinetic chromatography-tandem mass spectrometry (MEKC-MS/MS) has been developed for the identification and simultaneous quantification of thirteen benzimidazoles in animal urine. In order to obtain an appropriate separation with the highest sensitivity, different electrophoretic parameters … Continue reading
Posted in Anthelmintic, Benzimidazoles, Biological fluids, Dilute and shoot, Electrophoresis, MEKC, Mass spectrometry, P12-AGR-1647, Sweeping, Urine
Tagged CE, MS, stacking
Comments Off on Coupling sweeping-micellar electrokinetic chromatography with tandem mass spectrometry for the therapeutic monitoring of benzimidazoles in animal urine by dilute and shoot.
Characterization of carbamate pesticides in natural water from Cameroon.
With the increased use of chemicals in agriculture for crop protection and improvement of yield, the contamination of water is currently a serious health concern. This study used solid-phase extraction with ultra-high-performance liquid chromatography–tandem mass spectrometry to evaluate the presence … Continue reading
Posted in Carbamates, Mass spectrometry, P12-AGR-1647, Pesticides, SPE, UHPLC, Water
Tagged HPLC, MS, SPE
Comments Off on Characterization of carbamate pesticides in natural water from Cameroon.
Evaluation of hydrophilic interaction liquid chromatography–tandem mass spectrometry and extraction with molecularly imprinted polymers for determination of aminoglycosides in milk and milk-based functional foods.
An analytical method for the determination of eleven aminoglycosides in different types of milk and milk-based functional products has been optimized and validated. A hydrophilic interaction chromatography (HILIC) column was proposed for the separation of analytes by ultra-high performance liquid … Continue reading
Posted in AGL2015-70708-R, Aminoglycosides, HILIC, MIPs, Mass spectrometry, Milk, P12-AGR-1647
Tagged HPLC, MIPs, MS
Comments Off on Evaluation of hydrophilic interaction liquid chromatography–tandem mass spectrometry and extraction with molecularly imprinted polymers for determination of aminoglycosides in milk and milk-based functional foods.
Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
A selective and rapid method has been developed to determine 15 antibiotic residues (eight tetracyclines and seven quinolones) in milk samples by capillary zone electrophoresis coupled with quadrupole time-of-flight mass spectrometry (CZE-Q-TOF-MS). The use of this hybrid mass spectrometer allowed … Continue reading
Posted in Antibiotics, CZE, Food, Mass spectrometry, Milk, P12-AGR-1647, Quinolones, SPE, Tetracyclines
Tagged CE, MS, SPE
Comments Off on Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
A selective and rapid method has been developed to determine 15 antibiotic residues (eight tetracyclines and seven quinolones) in milk samples by capillary zone electrophoresis coupled with quadrupole time-of-flight mass spectrometry (CZE-Q-TOF-MS). The use of this hybrid mass spectrometer allowed … Continue reading
Posted in Antibiotics, CZE, Mass spectrometry, Milk, P12-AGR-1647, Quinolones, SPE, Tetracyclines
Tagged CE, MS, SPE
Comments Off on Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
