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Recent Posts
- Assessing human exposure to pesticides and mycotoxins: optimization and validation of a method for multianalyte determination in urine samples.
- Capillary electrophoresis tandem mass spectrometry to determine multiclass cyanotoxins in reservoir water and spinach samples.
- Determination of bile acids in serum of pigs exposed to polychlorinated biphenyls by liquid chromatography-mass spectrometry.
- Mycotoxin occurrence in milk and durum wheat samples from Tunisia using dispersive liquid–liquid microextraction and liquid chromatography with fluorescence detection.
- Deeper insights into the effects of low dietary levels of polychlorinated biphenyls on pig metabolism using gas chromatography-high resolution mass spectrometry metabolomics.
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Category Archives: Mycotoxins
Aspergillus section Flavi and aflatoxins in dried figs and nuts in Algeria
The presence of Aspergillus section Flavi and aflatoxin (AF) contamination was investigated in 112 samples of peanuts, almonds and dried figs collected in Algeria. The occurrence of aflatoxin B1 (AFB1), B2 (AFB2), G1 (AFG1) and G2 (AFG2) in different commodities has been determined with … Continue reading
Posted in AGL2015-70708-R, Aflatoxins, Dried fruit, HPLC, Mycotoxins, Nuts, Photo-induced, Solid-liquid extraction
Tagged Fluorescence, HPLC
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Determination of Fusarium toxins in functional vegetable milks applying salting-out-assisted liquid–liquid extraction combined with ultra-high-performance liquid chromatography tandem mass spectrometry
Vegetable milks are considered as functional foods due to their physiological benefits. Although the consumption of these products has significantly increased, they have received little attention in legislation with regard to contaminants. However, they may contain mycotoxins resulting from the … Continue reading
Posted in AGL2015-70708-R, Mass spectrometry, Mycotoxins, SALLE, UHPLC, Vegetable milks
Tagged MS, SALLE, UHPLC
Comments Off on Determination of Fusarium toxins in functional vegetable milks applying salting-out-assisted liquid–liquid extraction combined with ultra-high-performance liquid chromatography tandem mass spectrometry
Simple determination of aflatoxins in rice by ultra-high performance liquid chromatography coupled to chemical post-column derivatization and fluorescence detection
A fast and simple analytical method was developed and characterized for the determination of aflatoxins (B1, B2, G1 and G2) in rice. The procedure is based on a simple solid-liquid extraction without further clean-up, and analysis by ultra-high performance liquid … Continue reading
Posted in AGL2015-70708-R, Aflatoxins, Fluorescence, Rice, Solid-liquid extraction, UHPLC
Tagged Fluorescence, UHPLC
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Solid phase extraction as sample treatment for the determination of Ochratoxin A in foods: A review.
Ochratoxin A (OTA) is a mycotoxin produced by two main types of fungi, Aspergillus and Penicillium species. OTA is a natural contaminant found in a large number of different matrices and is considered as a possible carcinogen for humans. Hence, … Continue reading
Posted in Food, Mycotoxins, Review, SPE
Tagged SPE
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Development of magnetic molecularly imprinted polymers for selective extraction: determination of citrinin in rice samples by liquid chromatography with UV diode array detection.
In this work, we report the synthesis of novel magnetic molecularly imprinted polymers (m-MIPs) and their application to the selective extraction of the mycotoxin citrinin (CIT) from food samples. The polymers were prepared by surface imprinting of Fe3O4 nanoparticles, using … Continue reading
Posted in HPLC, MIPs, Mycotoxins, Rice, UV-vis
Comments Off on Development of magnetic molecularly imprinted polymers for selective extraction: determination of citrinin in rice samples by liquid chromatography with UV diode array detection.
Determination of aflatoxins in yogurt by dispersive liquid – liquid microextraction and HPLC with photo-induced fluorescence detection.
A high-performance liquid chromatography (HPLC) method with fluorescence detection for the determination of aflatoxins B1, B2, G1, G2, and M1 in yogurt using dispersive liquid–liquid microextraction as alternative sample treatment has been developed. To enhance the fluorescence of aflatoxins B1 … Continue reading
Posted in AGL2015-70708-R, Aflatoxins, DLLME, HPLC, P12-AGR-1647, Photo-induced, Yogurt
Tagged DLLME, HPLC
Comments Off on Determination of aflatoxins in yogurt by dispersive liquid – liquid microextraction and HPLC with photo-induced fluorescence detection.
Multiclass mycotoxin analysis in Silybum marianum by ultra high performance liquid chromatography–tandem mass spectrometry using a procedure based on QuEChERS and dispersive liquid–liquid microextraction
Ultra high performance liquid chromatography–tandem mass spectrometry (UHPLC–MS/MS) has been proposed for the determination of 15 mycotoxins in milk thistle (Silybum marianum), including aflatoxins, fumonisins, trichothecenes, ochratoxin A, citrinin, sterigmatocystin and zearalenone. The mycotoxins were detected by electrospray ionization in … Continue reading
Posted in DLLME, Mass spectrometry, Milk thistle, Mycotoxins, QuEChERS, UHPLC
Tagged MS
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Evaluation of dispersive liquid-liquid microextraction for the determination of patulin in apple juices using micellar electrokinetic capillary chromatography
Patulin (PAT) is a mycotoxin naturally found in fruits, including apples. Its occurrence as a natural contaminant of fruit juices is indicative of fruit quality in production. The European Union has set the maximum content of patulin in 50 μg/kg … Continue reading
Determination of ochratoxin A in wines by capillary liquid chromatography with laser induced fluorescence detection using dispersive liquid–liquid microextraction
A method based on reverse phase capillary high performance liquid chromatography (capillary HPLC) coupled to laser-induced fluorescence detection (LIF) has been proposed for the determination of ochratoxin A (OTA) in wine samples. An anionic micellar medium was added to the … Continue reading
Posted in Capillary HPLC, DLLME, LIF, Mycotoxins, Wine
Tagged HPLC
Comments Off on Determination of ochratoxin A in wines by capillary liquid chromatography with laser induced fluorescence detection using dispersive liquid–liquid microextraction