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Recent Posts
- Addressing chemical risks in beekeeping products: development of a combined ultrasound-assisted extraction and QuEChERS-based method for the simultaneous determination of mycotoxins and pesticides in bee pollen and honey.
- Toxic cyanopeptides monitoring in thermal spring water by capillary electrophoresis tandem mass spectrometry.
- Liquid chromatography-tandem mass spectrometry for the determination of multiple mycotoxins in serum through suspect screening and targeted approaches: Advancing human mycotoxin biomonitoring.
- Emerging mycotoxin occurrence in chicken feed and eggs from Algeria.
- HILIC-MS and CE-MS as complementary analytical approaches to assess the impact of exposure to polychlorinated biphenyls on the polar serum metabolome of pigs.
Tags
Tag Archives: MS
Evaluation of hydrophilic interaction liquid chromatography–tandem mass spectrometry and extraction with molecularly imprinted polymers for determination of aminoglycosides in milk and milk-based functional foods.
An analytical method for the determination of eleven aminoglycosides in different types of milk and milk-based functional products has been optimized and validated. A hydrophilic interaction chromatography (HILIC) column was proposed for the separation of analytes by ultra-high performance liquid … Continue reading
Posted in AGL2015-70708-R, Aminoglycosides, HILIC, MIPs, Mass spectrometry, Milk, P12-AGR-1647
Tagged HPLC, MIPs, MS
Comments Off on Evaluation of hydrophilic interaction liquid chromatography–tandem mass spectrometry and extraction with molecularly imprinted polymers for determination of aminoglycosides in milk and milk-based functional foods.
Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
A selective and rapid method has been developed to determine 15 antibiotic residues (eight tetracyclines and seven quinolones) in milk samples by capillary zone electrophoresis coupled with quadrupole time-of-flight mass spectrometry (CZE-Q-TOF-MS). The use of this hybrid mass spectrometer allowed … Continue reading
Posted in Antibiotics, CZE, Food, Mass spectrometry, Milk, P12-AGR-1647, Quinolones, SPE, Tetracyclines
Tagged CE, MS, SPE
Comments Off on Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
A selective and rapid method has been developed to determine 15 antibiotic residues (eight tetracyclines and seven quinolones) in milk samples by capillary zone electrophoresis coupled with quadrupole time-of-flight mass spectrometry (CZE-Q-TOF-MS). The use of this hybrid mass spectrometer allowed … Continue reading
Posted in Antibiotics, CZE, Mass spectrometry, Milk, P12-AGR-1647, Quinolones, SPE, Tetracyclines
Tagged CE, MS, SPE
Comments Off on Evaluation of a multiresidue capillary electrophoresis-quadrupole-time-of-flight mass spectrometry method for the determination of antibiotics in milk samples.
Validation of a new method based on salting-out assisted liquid-liquid extraction and UHPLC-MS/MS for the determination of betalactam antibiotics in infant dairy products
In this work a new multiresidue method has been developed for the determination of 15 betalactam antibiotics in infant milk and yogurt based on follow-on milk by ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS). The separation was achieved in 6 min, … Continue reading
Posted in Mass spectrometry, Milk, P12-AGR-1647, SALLE, UHPLC, Yogurt, β-lactams
Tagged HPLC, MS, SALLE
Comments Off on Validation of a new method based on salting-out assisted liquid-liquid extraction and UHPLC-MS/MS for the determination of betalactam antibiotics in infant dairy products
Determination of benzimidazoles in meat samples by capillary zone electrophoresis tandem mass spectrometry following dispersive liquid–liquid microextraction.
A novel method based on capillary zone electrophoresis-tandem mass spectrometry has been proposed and validated for the identification and simultaneous quantification of twelve benzimidazoles in meat samples. Electrophoretic separation was carried out using 500 mM formic acid (pH 2.2) as background … Continue reading
Posted in Benzimidazoles, CZE, DLLME, Mass spectrometry, P12-AGR-1647, Pork muscle
Tagged CE, DLLME, MS
Comments Off on Determination of benzimidazoles in meat samples by capillary zone electrophoresis tandem mass spectrometry following dispersive liquid–liquid microextraction.
High-throughput methodology for the determination of carbamates in food supplements by UHPLC–MS/MS.
Food supplements are increasingly consumed products that claim to have several benefits for health. In many cases, these supplements contain herbal products and, as a consequence, can be contaminated with pesticides used in crops. This study aimed to use a … Continue reading
Posted in AGL2015-70708-R, Carbamates, Mass spectrometry, QuEChERS, Supplements, UHPLC
Tagged HPLC, MS, QuEChERS
Comments Off on High-throughput methodology for the determination of carbamates in food supplements by UHPLC–MS/MS.
Evaluation of a new modified QuEChERS method for the monitoring of carbamate residues in high-fat cheeses by using UHPLC–MS/MS.
A simple and efficient method for the determination of 28 carbamates in high-fat cheeses is proposed. The methodology is based on a modified quick, easy, cheap, effective, rugged, and safe procedure as sample treatment using a new sorbent (Z-Sep+) followed … Continue reading
Posted in Carbamates, Cheese, Mass spectrometry, P12-AGR-1647, QuEChERS, UHPLC
Tagged HPLC, MS, QuEChERS
Comments Off on Evaluation of a new modified QuEChERS method for the monitoring of carbamate residues in high-fat cheeses by using UHPLC–MS/MS.
Salting-out assisted liquid–liquid extraction coupled to ultra-high performance liquid chromatography–tandem mass spectrometry for the determination of tetracycline residues in infant foods
The use of salting-out assisted liquid–liquid extraction (SALLE) combined with ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC–MS/MS) has been evaluated for the determination of tetracyclines in infant foods based on meat and vegetables or in milk. To obtain satisfactory … Continue reading
Posted in Infant foods, Mass spectrometry, P12-AGR-1647, SALLE, Tetracyclines, UHPLC
Tagged MS
Comments Off on Salting-out assisted liquid–liquid extraction coupled to ultra-high performance liquid chromatography–tandem mass spectrometry for the determination of tetracycline residues in infant foods
QuEChERS-based method for the determination of carbamate residues in aromatic herbs by UHPLC-MS/MS
A new reliable, fast and highly sensitive method based on ultra-high performance liquid chromatography tandem mass spectrometry has been developed and validated for the determination of 28 carbamates in aromatic herbs. A modified QuEChERS-based method was optimized for the extraction … Continue reading
Posted in AGL2015-70708-R, Aromatic herbs, Carbamates, Mass spectrometry, QuEChERS, UHPLC
Tagged MS
Comments Off on QuEChERS-based method for the determination of carbamate residues in aromatic herbs by UHPLC-MS/MS
Rapid and simple UHPLC-ESI-MS/MS method for the screening of propyl propane thiosulfonate, a new additive for animal feed
Allium derivative propyl propane thiosulfonate (PTSO) is a new additive for animal feed which improves animal health when used as an alternative to antibiotic growth promoters. Despite the effort of the European Union to ensure the control of animal feed … Continue reading
Posted in Animal feed, Mass spectrometry, PTSO, UHPLC
Tagged MS
Comments Off on Rapid and simple UHPLC-ESI-MS/MS method for the screening of propyl propane thiosulfonate, a new additive for animal feed
